UHV Chamber

What is my research?

Throughout the blog, I have often talked about the fact I do scientific research as part of my PhD. However, I wanted to take this blog post as an opportunity to actually explain what my area of research is and how I do it. I got this idea when talking to people at my accommodation who I have probably bored with work stories (sorry about that). I realized they have no context to what I am saying and have not had the chance to see the equipment I get to use!

I will start by explaining that my research uses ultra-high vacuum (UHV) chambers and inside these is a surface that allows us to mimic an interstellar gain. You can see more about UHV chambers in this video so I will not explain them any further in this blog post.

When I first arrived, I spent my time working with Frederik and Rijutha helping them with their research while learning how to use a UHV chamber and the different methods we can use to investigate reactions in interstellar space. At the beginning of this month, I stopped helping Frederik and have been able to start my own experiments. I aim to investigate putting glycine onto a surface and then exposing it to hydrogen to see what reactions occur. Believe me this sounds much easier than it actually is and I will explain why I am doing this, what glycine is and how I have been/plan to do this. I have been using the Big Chamber, which you can read more about here or just look at this photo of it.

The Big Chamber

Glycine is an amino acid, which are known as building blocks of life. They are called this as they are the simplest component that joins together to form proteins that organisms need for life to function. Discovering if these molecules can form and then survive in the conditions found in interstellar space is necessary to answer the question of how life first originated. Hydrogen is found in these conditions and so seeing how it reacts with amino acids is a crucial component. I chose glycine as it is the simplest of the amino acids and so it is the easiest to form. You can see below what the structure of a single glycine molecule looks like.

Glycine Molecule

I have put the glycine into a molecular doser which heats the glycine and causes it to be deposited onto the surface (step 1 in the figure below). It builds up on the surface to form a multilayer, which means it assembles into several layers. I then heat the surface causing all the layers apart from the first to be removed. This layer remains due to its stronger interactions with the surface. This single layer of glycine is called a monolayer and is the step I am currently at.

After I successfully do this I will expose the surface to the hydrogen for varying periods of time (step 2 in the figure below). Now I need a way of finding out what I have formed. To do this I am using a temperature programmed desorption which I have talked about before but is simply heating the surface such that the molecules desorb (are released from) the surface where I can then detect them using a mass spectrometer (step 3 in the figure below). I hope to see that the hydrogen has bonded to the glycine to form a radical and its mass is increased by one hydrogen mass.

The process of a Temperature Programmed Desorption (TPD) measurement.

I will be doing more than just this for the next four years and I will use different techniques but it is a good feeling to have started on my own research! I now just need to do what I have said I will do in this blog post but I can assure you after being stuck in the UK for months being unable to do the experimental research I wanted it is very enjoyable to feel like I am progressing onto the real science work.

Posted by Alfred Hopkinson in Alfie&Julia, 0 comments

Getting to grips with my ‘new normal’

I don’t know about you Julia, but Denmark is a very different world to the one I have left in the UK. Here they have done much better in their fight against Covid and there are a lot more things you can safely do. I have even been able to get a negative test and go into the university to see the members of InterCat who are yet to go on vacation! This isn’t the only difference, the weather has been sunny and hot (which I am told isn’t typical of Denmark, but I am enjoying it regardless) and I am getting to experience Danish food.

During the first week and a half I have been allowed out of my room, I have been trying to settle in and get used to my new surroundings. I am currently in student accommodation, which is vastly different to British halls of residence. These dormitories have pleasant living room kitchens where people play games, party or make a big group meal. It is a good way to meet people and build a community spirit and I as an incomer have really appreciated it. I will say I was surprised at the quality of the food, the things people make are much nicer than many of the meals I have seen in British student accommodation…

July was an odd time to arrive as many people have just gone on vacation and so my accommodation was quite quiet but I have still met a few housemates who have been very welcoming. Although I will freely admit to being jealous of them being able to enjoy the nice weather by going to the beach or taking a boat trip while I was at the university. They have helped me with a variety of different issues and have been teaching me some more Danish. I can now say jeg spiser æbler og drikker øl eller vand. (It isn’t that versatile but has its uses)

Julia asked me if I had seen any interesting facilities in her last post and the answer is yes. I have really made an effort to go into the university and spend time in the laboratory for astrochemistry and reactions on surfaces. This is where we have some of the ultra-high vacuum chambers (UHV) and has provided me with many opportunities to look at some interesting physics. I have been helping Frederik with his work before he goes on vacation which has required me to learn how to do a temperature programmed desorption (you can see what this is here) on a  UHV chamber (specifically the big chamber).

Working on the big chamber with Frederik and Georgios

I have now almost learnt how to do this and over the next week have the opportunity to do it on my own and put my newfound knowledge to the test! For the rest of the summer I will aim to do a wide mix of different activities such as making a poster for the InterCat retreat and discussing with John about how to incorporate a Fourier Transform Infrared spectrometer (FTIR) into my research. The plan is to try to learn as much as I can during these summer months so in September I can hit the ground running and make up for lost time! Do you have any aims for the summer Julia other than getting ready for the cold winters of Europe?

Posted by Alfred Hopkinson in Alfie&Julia, 0 comments